Microwave Assisted Synthesis of N-Benzylenaminones Catalyzed by Chloroacetic Acid

Document Type: Research Paper

Authors

Department of Chemistry, Yadegar-e-Imam Khomeini (RAH) Shahre-rey Branch, Islamic Azad University, Tehran, Iran

Abstract

Benzylaminoalkenones and benzylaminoalkenoates 3 were synthesized from reaction of benzylamine with corresponding 1,3-diketones and 1,3-ketoesters in the presence of catalytic amount of chloroacetic acid under microwave radiation. This method offers several advantages including high yield of products, recyclable of the catalyst and easy experimental work-up procedure.

Keywords

References

1- A-Z. A. Elassar, A. A. El-Khair, Tetrahedron, 59 (2003), 8463.
2- P. Simunek, V.Machácek, Dyes and Pigments, 86 (2010), 197.
3- A.R. Khosropour, M.M. Khodaei, M. Kookhazadeh, Tetrahedron Lett. 45 (2004), 1725.
4- A.R. Gholap, N.S. Chakor, T. Daniel, R.J. Lahoti, K.V. Srinivasan,Journal ofMolecular Catalysis A: Chemical, 245 (2006), 37.
5-B. Giuseppe, B. Marcella, L. Manuela, M. Enrico, M. Paolo, S. Letizia, Synlett, (2004), 239.
6-M. Kidwai, S. Bhardwaj, N.K. Mishra, V. Bansal, A. Kumar, S. Mozumdar, Catalysis Communications, 10 (2009) 1514–1517.
 
7- M.A.P. Martins, C.P. Frizzo, D.N. Moreira, F.A. Rosa, M.R.B. Marzari, N. Zanatta, H.G. Bonacorso, Catalysis Communications, 9 (2008), 1375.
8-I. Yavari, A.S. Shahvelayati, Phosphorus, Sulfur, and Silicon, 185 (2010), 1726.
9-I. Yavari, M. Ghazvini, A.S. Shahvelayati, M.M. Ghanbari, Phosphorus, Sulfur, and Silicon, 186 (2011), 134.
International Journal of New Chemistry

Volume 1, Issue 4
Autumn 2014
Pages 145-150

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